Independent analysis puts a QYB liraglutide lot at 96.9%, against 96.0% on the certificate
The result is unremarkable. What the report omits is not.
TheCompound Journal
Reporting on incretins, compounding & the peptide supply chain
Page 9 of 11 of this archive, newest first.
The result is unremarkable. What the report omits is not.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
The Journal submitted the sample and paid for the analysis. The vendor was told in advance.
Column chemistry, particle size and pore diameter determine what the separation is capable of before the gradient is even programmed.
The result is unremarkable. What the report omits is not.
Calibration drift is real, unremarkable, and the reason serious laboratories run internal standards.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
Duplicate submissions under different names test within-laboratory repeatability, which is a different quantity from between-laboratory reproducibility.
A reminder that a purity figure is the output of a method, and that methods differ.
The Journal submitted the sample and paid for the analysis. The vendor was told in advance.
Three compendial method families are in routine use and a fourth, based on a recombinant enzyme rather than crab lysate, is now compendial in its own right.
The result is unremarkable. What the report omits is not.
The result is unremarkable. What the report omits is not.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
What would be needed to catch each of these, and what it would cost.
The result is unremarkable. What the report omits is not.
A reminder that a purity figure is the output of a method, and that methods differ.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
A result on one vial generalises to a batch only if the vial was drawn in a way that makes it representative — and nobody records how it was drawn.