PeptideMeter result on a Guangzhou exenatide lot lands 4.3 points below the supplier’s figure
The result is unremarkable. What the report omits is not.
TheCompound Journal
Reporting on incretins, compounding & the peptide supply chain
Page 4 of 6 of this archive, newest first.
The result is unremarkable. What the report omits is not.
A shallow gradient resolves impurities that a steep one runs into the parent peak. Both methods are legitimate; only one of them can see the small stuff.
A reminder that a purity figure is the output of a method, and that methods differ.
The header identifies the batch, the table records the tests, and the footer says who is answerable. Two of the three are usually incomplete.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
We asked all four services what they can determine, on what timescale, at what price, and under what accreditation. The answers are printed in full.
The Journal submitted the sample and paid for the analysis. The vendor was told in advance.
The Journal submitted the sample and paid for the analysis. The vendor was told in advance.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
Two years ago we ran an anonymised version of this comparison and promised a named one. This is it, with every method printed in full.
The result is unremarkable. What the report omits is not.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
The Journal submitted the sample and paid for the analysis. The vendor was told in advance.
The Journal submitted split samples from single lots to three assay services, under names unconnected to this publication, and published each method alongside each result.
We submitted vials for endotoxin determination and report the results, the method and the laboratory, because a pyrogen figure without a method is as empty as a purity…
Calibration drift is real, unremarkable, and the reason serious laboratories run internal standards.
The report states the gradient, the wavelength and the integration threshold, which is more than most.
A reminder that a purity figure is the output of a method, and that methods differ.
A reminder that a purity figure is the output of a method, and that methods differ.
A badge asserts that something was tested. It does not assert what, when, on whose sample, by what method, or whether the lot on sale is the lot that was tested.